GREEN SYNTHESIS AND CHARACTRISATION OF NOVEL TRIAZOLES DERIVATIVES OF 2-MERCAPTOBENZOTHIAZOLE
Mathapati Sushil Ramakant*, Vhadlure Amit Nillappa, Kalalawe Virbhadra Gangadhar, Swami Mantosh Bhimashankar, Ghuge Hanumant Gunaji, Dawle Jairaj. Kishanrao
ABSTRACT
Novel 2-Mercaptobenzothiazole deriveties synthesized
from 2- Mercaptobenzothiazole reacted with ethyl chloroacetate to get
ester derivatives (3) using Green method. These ester converted to
hydrazids (4) by reaction with hydrazine hydrate under MWI. 5-
substituted 1,3,4-oxadiazole (5a-g) synthesized from hydrazide,
substituted benzoic acid and phosphprous oxochloried by Microwave
irradiation as reported in literature.1,3,4- Triazoles 6a-g synthesized
from above oxadiazole 5a-g. The structure of newly synthesized
compound was established by physico-chemical and spectral data
analysis.
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